Reductive cleavage of 1,3-dioxanes 1a-c with Li metal in the presence of a catalytic amount of naphthalene in THF, followed by reaction with different electrophiles, allowed the synthesis of 3-substituted- and 3, 3-disubstituted-3-phenylpropan-1-ols 4 in good yields
Generation of g-Oxy-Substituted Benzyllithium Derivatives by Reductive Lithiation of 4-Phenyl-1,3-dioxanes / Azzena, Ugo Gavino; Luciano, Pilo. - In: SYNTHESIS. - ISSN 0039-7881. - (1999), pp. 664-668.
Generation of g-Oxy-Substituted Benzyllithium Derivatives by Reductive Lithiation of 4-Phenyl-1,3-dioxanes
AZZENA, Ugo Gavino;
1999-01-01
Abstract
Reductive cleavage of 1,3-dioxanes 1a-c with Li metal in the presence of a catalytic amount of naphthalene in THF, followed by reaction with different electrophiles, allowed the synthesis of 3-substituted- and 3, 3-disubstituted-3-phenylpropan-1-ols 4 in good yieldsFile in questo prodotto:
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